The Smell of Molten Projects in the Morning

Ed Nisley's Blog: Shop notes, electronics, firmware, machinery, 3D printing, laser cuttery, and curiosities. Contents: 100% human thinking, 0% AI slop.

Category: Science

If you measure something often enough, it becomes science

  • Poughkeepsie Waterfront at Night

    Another Walkway Over the Hudson Moonwalk provided a good view of the Poughkeepsie waterfront:

    City of Poughkeepsie Waterfront - night view
    City of Poughkeepsie Waterfront – night view

    The railroad station’s parking garage produces the big mass of sodium light in the middle and (I think) the bleached church on the far left has mercury vapor floodlights.

    The smaller spots of cold-white LED lighting scattered here-and-there will gradually expand and, in five years or so, take over the entire vista …

  • Cast Iron Pan Seasoning

    The motivation for stripping our cast iron pans:

    Wagner cast iron skillet - before - top
    Wagner cast iron skillet – before – top

    The bottom, of course, carried a heavier layer of crust:

    Wagner cast iron skillet - before - bottom
    Wagner cast iron skillet – before – bottom

    The wet areas came from the usual after-breakfast washing.

    Looking down into the electrolytic stripping bath, with bubbles forming on exposed metal areas around the crust on the bottom of the pan:

    Wagner cast iron skillet - in stripping bath
    Wagner cast iron skillet – in stripping bath

    After a day of electrolysis, all the crust was gone. Low labor, low danger, no fuss, not much muss.

    Given three stripped pans, the seasoning process involved wiping them with flaxseed oil, baking at 500 °F for an hour, cooling for two hours, and repeating. Six iterations occupied a long day, uncomfortably warmed the kitchen during a long hot summer day, and turned out to be just fussy enough to fit around some short-attention-span projects.

    Fast forward one day.

    The outside of the seasoned pans looks lovely:

    Wagner cast iron skillet - after - bottom
    Wagner cast iron skillet – after – bottom

    I’d have been hard-pressed to pick out the “Wagner Ware” before stripping the pan.

    The inside of all three pans had a peculiar mottled appearance:

    Wagner cast iron skillet - after - top
    Wagner cast iron skillet – after – top

    The medium pan:

    Medium cast iron pan - after - top
    Medium cast iron pan – after – top

    The small pan:

    Small cast iron pan - after - top
    Small cast iron pan – after – top

    The dark spots might suggest I used too much oil and it puddled / collected / whatever while baking, except that I’d slathered the oil on using a scrap from a cotton towel (actually, many scraps, one per iteration), then wiped it off with more towel scraps before baking the pans.

    Protip: You’ll eventually have a pile of cotton rags soaked in a drying oil similar to linseed oil. Woodworkers will tell you to wet oily rags with water before sealing them in a plastic bag, because the “drying” process is exothermic: oil-soaked rags can get hot enough for spontaneous combustion. Make it so.

    Breakfast proceeded pretty much as usual and the giant omelet (5 eggs, lots of chopped chard, two finely chopped bacon rashers, cheddar cheese, plenty of oil, stuff like that) seemed to stick somewhat less than usual: it’s not a Teflon-coated pan, but worked pretty well.

    I did the usual post-breakfast KP, which involves washing the pan with ordinary dish soap, scuffing the recalcitrant bits, and dropping the pan in the dish drainer. I don’t scour the pans, but I don’t treat them with fawning obeisance, either; they’re utensils, not sacred objects.

    Just before lunch, this appeared:

    Wagner cast iron skillet - washed - top
    Wagner cast iron skillet – washed – top

    The bottom sported similar rust spots:

    Wagner cast iron skillet - washed - bottom
    Wagner cast iron skillet – washed – bottom

    So that suggests I didn’t apply enough oil. Or scrubbed too hard. Or did something utterly wrong.

    Haven’t a clue about what happened. If I didn’t follow the seasoning process, I don’t know what I’d change. Ditto for washing up; it’s not like we haven’t been using the pan for decades.

    After supper, I washed & dried the pan, slathered on a generous oil coating, and let it sit, all in the hope the oil eventually forms a good crusty layer.

    By and large, the pan works better than it did before and the seasoning not nearly as well as I expected.

  • Diurnal Pumping, Fluid Division

    I caught this just before it made a mess:

    Sta-Bil jar - diurnal pumping
    Sta-Bil jar – diurnal pumping

    That container lives in the garage, where the air temperature pretty much tracks the weather.

    When the air in the main compartment heats up, it pushes fluid up into the dispensing compartment. Although both caps were screwed on finger-tight, apparently the smaller cap leaks just enough that the pumped fluid can push the air out through the not-so-good seal.

    Another few weeks and it’d be sitting in a puddle!

  • Monthly Science: Sony NP-BX1 Battery Status

    Having had the weaker of the two surviving STK batteries die 36 minutes into a ride, I tested them all:

    Sony NP-BX1 - 1 A test - 2016-08-17
    Sony NP-BX1 – 1 A test – 2016-08-17

    The X axis shows W·h, rather than the usual A·h, because that seems more useful in a world of constant-power supplies.

    The test current is now 1 A, rather than the previous 500 mA, to more closely match the camera’s actual load. The CBA tester doesn’t have a constant-power mode; I think that doesn’t make much practical difference.

    The orange curve (STK D) is the failed battery, ending after 1.4 W·h. At an average 3.2-ish V, that’s 26 minutes, which is close enough to the actual run time, given the different current.

    The red curve (STK C) is the sole STK battery of the original four from last November that actually worked.

    The upper two curves come from the mostly unused Wasabi batteries (F and G), also from November. They have lost a bit of their capacity, but show the highest voltage out toward the end, so that’s good.

    The black curve is the lightly used Sony OEM battery that came with the camera. Although it has about the same ultimate capacity as the other three “good” batteries, the voltage depression suggests it’ll trip out early.

    The others are pretty much debris by now. I suppose they might be good for LED blinkies or some other low-voltage and low-current application, but …

    So I’ll start using all four of the better batteries and see how the run times work out in actual use.

  • LF Loop Antenna: GPS Frequency Check

    I stuck some old 12 V 7 A·h batteries in my homebrew power supply for the HP 3801A GPS Time / Frequency Standard, fired it up, put the antenna where it could see a good chunk of the sky, gave it a day to warm up / settle out, and it’s perfectly happy:

    ------------------------------- Receiver Status -------------------------------
    
    SYNCHRONIZATION ............................................. [ Outputs Valid ]
    SmartClock Mode ___________________________   Reference Outputs _______________
    >> Locked to GPS                              TFOM     3             FFOM     0
       Recovery                                   1PPS TI -38.3 ns relative to GPS
       Holdover                                   HOLD THR 1.000 us
       Power-up                                   Holdover Uncertainty ____________
                                                  Predict  366.2 us/initial 24 hrs
    
    ACQUISITION ............................................ [ GPS 1PPS CLK Valid ]
    Satellite Status __________________________   Time _____ +1 leap second pending
    Tracking: 4        Not Tracking: 6            UTC      18:22:19     22 Jul 2016
    PRN  El  Az   SS   PRN  El  Az                1PPS CLK Synchronized to UTC
      3  34 104   48   * 1  36  48                ANT DLY  0 ns
     17  62 308  103     6  27 220                Position ________________________
     19  39 281   50    11  21  58                MODE     Hold
     28  80 133   64   *22  Acq .
                        24  12 319                LAT      N  41:39:32.328
                        30  15 191                LON      W  73:52:26.733
    ELEV MASK 10 deg   *attempting to track       HGT               +82.87 m  (MSL)
    HEALTH MONITOR ......................................................... [ OK ]
    Self Test: OK    Int Pwr: OK   Oven Pwr: OK   OCXO: OK   EFC: OK   GPS Rcv: OK
    scpi >
    

    The FFOM 0 entry says the Frequency Figure Of Merit is “within specifications” of 10-9, averaged over one day. That means the actual frequency should be within 0.010 Hz of 10 MHz.

    Feeding the 10 MHz frequency reference into the (equally warmed up) HP 8591E spectrum analyzer and selecting an absurdly narrow span produces a comforting sight:

    HP Z2801A GPS Receiver - 10 MHz ref - HP 8591E
    HP Z2801A GPS Receiver – 10 MHz ref – HP 8591E

    Given the horizontal resolution, that’s dead on 10 MHz.

    So, yeah, that signal at 57-ish kHz really isn’t at 60.000 kHz:

    Loop - 40T 1nF - spectrum
    Loop – 40T 1nF – spectrum

    Which is good to know …

  • LF Loop Antenna: 60 kHz Tuning

    The object of soldering all 40 wires in the 5 m hank of ribbon cable  in series is to build a 40 turn loop antenna to receive LF radio signals like WWVB at 60 kHz. The antenna, being basically a big coil of wire, will have an inductance that depends on its layout, so putting a capacitor in parallel turns it into a resonant tank circuit. Given a particular layout (and, thus, an inductance), you can choose the capacitor to make the antenna resonant at whatever frequency you need (within reason).

    With the joints soldered & reinforced with epoxy, the inductance across all 40 turns:

    • 535 µH – rolled into a compact bundle
    • 6.66 mH – vaguely circular loop on the concrete floor
    • 5.50 mH – lumpy rectangle on the concrete floor

    Back in a slightly different circular layout on the floor:

    • 6.8 mH – across all 40 turns, as above
    • 2.0 mH – across either set of 20 turns from the center tap

    Given that inductance varies as the square of the number of turns, you’d expect a factor of four between those two inductances, but that’s not how it worked out.

    Hanging the loop from a pair of screws in the floor joists to make a droopy rectangle-oid shape and driving it from a 600 Ω signal generator through a 10 kΩ resistor, it’s self-resonant at 213 kHz. Repeating that with a 470 kΩ resistor drops the resonance to 210 kHz, which isn’t different enough to notice and surely has more to do with my moving the loop while dinking with resistors.

    Adding parallel capacitance (measured with an LCR meter, just to be sure) changes the resonance thusly:

    • 9.9 nF → 20 kHz
    • 900 pF → 64 kHz
    • 400 pF → 87 kHz
    • 250 pF → 108 kHz
    • none → 213 kHz

    Because the resonant frequency varies inversely as the square root of the capacitance, halving the resonant frequency means you’ve increased the capacitance by a factor of four. Because 250 pF halves the frequency (mostly kinda sorta close enough), the loop’s stray capacitance must be about 1/3 of that: 83 pF.

    Yeah, 1/3, not 1/4: the additional capacitance adds to the stray capacitance, so it goes from 83 pF to 250 + 83 pF = 333 pF, which is four times 83 pF.

    (If that sound familiar, it’s similar to the resonant snubber calculation.)

    The self-resonant frequency of 213 kHz and the 83 pF stray capacitance determines the loop inductance:

    L = 1/((2π · 213 kHz)^2 · 83 pF) = 6.9 mH

    Pretty close to the measured value from the floor, I’d say.

    To resonate the antenna at 60 kHz, the total capacitance must be:

    60 kHz = 1/(2π · sqrt(6.9 mH · C)) → C = 1050 pF

    Which means an additional 1050 – 83 =  970-ish pF should do the trick, which is about what you’d expect from the 64 kHz resonance with the 900 pF cap above. I paralleled pairs of caps until it resonated at 59.9 kHz.

    The -3 dB points (voltage = 1/sqrt(2) down from the peak) turned out to be 58.1 and 60.1 kHz, so my kludged caps are slightly too large or, once again, I nudged the loop.

    Figuring Q = (center frequency) / bandwidth = 59.1 / 2 = 30, which works out close enough to Q = X / R = 2600 / 80 = 33 to be satisfying. Using standard 26-ish AWG ribbon cable, rather than crappy 31-ish AWG eBay junk, would double the conductor area, halve the series resistance, and double the Q. Faced with that much resistance, I’m not sure better caps would make any difference.

    Attaching the spectrum analyzer through a 470 Ω resistor to reduce the load:

    Loop - 40T 1nF - spectrum
    Loop – 40T 1nF – spectrum

    I’d love to believe that big peak over on the left at 57.1 kHz is WWVB, but it’s not.

    What’s more important: the broad hump between 56 and 62 kHz, where the increased amount of background hash suggests the antenna really is resonant, with a center frequency around 59 kHz. The -3 dB points might be 57 and 61 kHz, but at 10 dB/div with 5 dB of hash, I’d be kidding myself.

    Dang, I love it when the numbers work out!

    It’s faintly possible the spectrum analyzer calibration is off by 2.5 kHz at the low end of its range. The internal 300 MHz reference shows 299.999925 and it puts FM stations where they should be, but the former could be self-referential error and the latter lacks enough resolution to be comforting. I must fire up the GPS frequency reference, let it settle for a few days, see whether it produces 10.000000 MHz like it should, then try again.

    The original measurements:

    Loop antenna tuning - measurements
    Loop antenna tuning – measurements
  • Monthly Image: Helmet Camera vs. Water Droplets

    Riding into the Village of Wappingers Falls, there’s a lumpy patched pothole just ahead of the fairing & front wheel:

    Water Droplets - 2016-07-19 - 0196
    Water Droplets – 2016-07-19 – 0196

    You can watch (and I can hear) the fairing flex as the front end jounces over the patch:

    This slideshow requires JavaScript.

    The hydration pack slung behind the seat also jounces and, when the reservoir bag bottoms out, the sudden pressure increase squirts water out of the bite valve, all over my face and goggles, and way out in front of the camera:

    This slideshow requires JavaScript.

    The camera runs at 60 images/second: those 28 images span all of 450 ms.

    Two seconds later, the droplet stabilized into a nice round lens:

    Water Droplets - 2016-07-19 - 0360
    Water Droplets – 2016-07-19 – 0360

    The low humidity of a lovely day evaporated the drop after another three minutes…