Ed Nisley's Blog: Shop notes, electronics, firmware, machinery, 3D printing, laser cuttery, and curiosities. Contents: 100% human thinking, 0% AI slop.
Having accumulated a bunch of used activated alumina desiccant, I figured now was a good time to try regenerating it. Industrial applications use dry gas and very high temperatures, but perhaps holding it over 100 °C for a few hours will suffice for my purposes.
After an hour the surface temperature was around 150 °F, so I covered the pan with a water-cooled lid to see if any vapor condensed on it:
Alumina regeneration – lid cooling
It did, indeed, so I alternated covering and exposing the pan, which was likely a waste of my time, until the alumina dried enough that the lid didn’t collect any condensation. The whole process took just under four hours with the cooktop set to its maximum of 460 °F for most of the time.
The beads then cooled to room temperature in a covered dish:
Alumina regeneration – final cooling
The beads weighed 626 g at the start of the adventure and sweated down to 593 g, parting with 33 g = 1.2 oz of water in the process for a loss of 5.6%. I have no idea how dry they are now, but they’re an ounce drier than before.
The upstairs Sewing Room came with a couch-like bed incorporating a roll-out trundle bed. It doesn’t get a lot of use, but it lacks wheel locks and tends to scoot away unless you get into it rather more carefully than seems reasonable.
So I made a pair of stops to capture the wheels:
Rolling Bed Stops – installed
The solid model shows they’re just plastic blocks minus a model of the roller wheel:
Rolling Bed Stops – solid model – show view
I like the wood-grain effect of the doubly curved recess on printed plastic layers, even if nobody will ever see it:
Rolling Bed Stops – PrusaSlicer
The OpenSCAD code also exports a projection of the block as an SVG file to laser-cut the cork pad.
Roll the trundle bed into position, push the stops against the wheels, lift and pull forward an inch, let it down, and the wheels snap into those recesses.
These are considerably fancier than some of the other wheel stops / feet around the house, if only because I got to use the Chord Equation to solve for the radius of the circle parallel to the axle for a snug socket.
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The indicator cards show the humidity is maybe a little over 10 %RH:
PolyDryer – TPU base – 10pctRH cards
The meter jammed in the other end of the box splits the difference at 15 %RH:
PolyDryer – TPU base – 15pctRH TP
Put the box atop the improved PolyDryer, set it for the recommended 12 hours with “two bars” of oomph (which may roughly correspond to the temperature), and fire it up.
The OEM meter occasionally glitches to 10 %RH:
PolyDryer – TPU dry 1200h – 10pctRH glitch OEM
That type of humidity meter apparently reports values from 10 %RH upward, so this seems like the kind of glitch where the reading jams at one end of the range due to the sensor opening up / shorting / misbehaving. It does not correlate with any nearby electrical activity due to fans / heaters / 3D printers / whatever.
A little under eight hours later, it shows 17 %RH:
PolyDryer – TPU dry 0425h – 17pctRH OEM
Although it still has glitches to 10 %RH.
The cards look about the same, although I could be persuaded the 10% spots look ever so slightly more blue:
PolyDryer – TPU dry 0425h – 10pctRH cards
The meter in the back shows it’s toasty in there:
PolyDryer – TPU dry 0425h – 10pctRH TP
A psychrometric chart shows heating air from 66 °F & 15 %RH to 117 °F will put it at 3 %RH without removing any water vapor. This is far below the level my cheap “instrumentation” can measure, but it does suggest the meters should bottom out, regardless of whatever the silica gel is doing.
Allowing six hours to cool down & stabilize after the PolyDryer turns off in the middle of the night (because for science does not include all-nighters) shows a rebound to 26 %RH on the OEM meter:
PolyDryer – TPU dry 0000h – 26pctRH OEM
The cards remain unchanged:
PolyDryer – TPU dry 0000h – 10pctRH cards
The meter in the back again splits the difference at 16 %RH:
PolyDryer – TPU dry 0000h – 16pctRH TP
I pulled the larger meter and both cards out of the box.
After sitting undisturbed for a day, the OEM meter in the box stabilized at 10 %RH:
PolyDryer – TPU post dry – 10pctRH OEM
The card agrees, to the best of its limited resolution:
PolyDryer – TPU post dry – 10pctRH card
The silica gel weighs 25.0 g, exactly what it did when I loaded the meter case. I think the scale’s 0.1 g resolution exceeds its accuracy, but even if the silica gel weighed 25.2 g ≅ 0.8 % water the humidity would be under 5 %RH.
As far as I can tell:
The filament on the spool isn’t outgassing water vapor
The air in the TPU box remains under 15-ish %RH at normal basement temperature
Running a PolyDryer cycle at 15-ish %RH doesn’t stuff any more water vapor in the silica gel
Cheap humidity meters lack accuracy around 15-ish %RH
Humidity meters take longer than you think to stabilize
Humidity indicating cards may be as good as you (well, I) need
With the nose ring lights in place, I soldered up eight more 24 V LED strips to light the quilt under the HQ Sixteen’s arm:
HQ Sixteen – under-arm lights – bottom view
A simple fixture aligned the strips for soldering:
HQ Sixteen – under-arm lights – soldering fixture
I intended to peel the masking tape off the glossy cardboard, then use it to keep the strips aligned while I pressed the PSA adhesive on the back of the strips to the machine. The silicone molded over the LEDS turned out to be supremely un-stick-able to the tape and the strips got far more handling than I planned, but I think the adhesive will work.
The cable from the power supply now has a pair of JST SM connectors on the end. Although crimping two conductors into the same pin is not good practice, all 14 of the LED strips draw an aggregate of maybe 130 mA, so I think it’ll suffice.
The JST connectors hide behind the ribbon cable going to the machine’s front panel, so there’s not a lot of basis for arguing they’re unsightly:
HQ Sixteen – under-arm lights – side view
The finished part of the quilt passes under the bottom bar on the left (the rear of the machine table) and forms an ever-increasing roll around the top bar; the white fabric leader attaches to the edge of the quilt. The LED strips illuminate the in-progress part of the quilt under the arm and should be far enough forward to not snag on the rolled-up finished part.
An adjacent pair of PolyDryer boxes have black and orange PETG filament:
PolyDryer – PETG – 27 pctRH Black 25 pctRH Orange
They’ve been sitting closed up for a week or so, with only 25 g of activated alumina in the desiccant holder (no tea bags with additional desiccant) pulling moisture out of their air and, presumably, filament.
The desiccant from the black filament weighed 29.0 g, showing it pulled 4.0 g of water out of the air, 16% of its original weight.
The “aluminum oxide” curve shows 16% adsorption should correspond to more than 50% RH, so the numbers don’t quite match up. On the other paw, I don’t know how much I can trust the meter accuracy.
I replaced the desiccant with 25 g of silica gel, tucked a humidity indicating card into the box, and snapped it closed again. The orange PETG box also got an indicating card so I can compare results.
The OEM fan inside the PolyDryer is annoyingly loud, even to my deflicted hearing, so I printed a Noctua NF-A4x10 fan adapter and installed a much quieter fan:
PolyDryer – Noctua fan installed
The adapter is upside-down from the suggested orientation, I didn’t bother screwing it to the fan because it has sleeves fitting into the fan screw holes, the slot holds everything together, the vivid green EVA foam sheet sits atop a craft adhesive sheet (both cut with scissors!) ensuring they don’t part company, and it works just fine.
Of course, the OEM fan has a three-wire cable and the Noctua has a four-wire cable:
PolyDryer – OEM vs Noctua fan cables
Although you can’t quite make it out on the white plastic, both connectors have their Pin 1 marks adjacent to each other. I oriented them like that to put the pin release latches on top; a foolish consistency is the hobgoblin of small minds.
Fortunately, Noctua documents their pinout, a bit of probing verified the OEM fan pinout (which does not match the Noctua 3-wire pinout), and the Basement Warehouse Wing emitted an assortment of matching JST XHP connectors. Chop off the black connector and rewire it in a 3-pin XHP connector:
Pin 1 = OEM Red → Noctua Yellow = +24 V
Pin 2 = OEM Yellow → Noctua Green = Tachometer
Pin 3 = OEM Black → Noctua Black = Ground / Common
unused = Noctua Blue = PWM Speed Control
Which is barely visible plugged into the control PCB on the left:
PolyDryer – Noctua fan wiring
The brown thermocouple wire in the upper right didn’t start out in the notch intended to pass it out of the air flow downwind of the heater:
PolyDryer – crunched thermocouple wire
The wire is exceedingly stiff and requires some persuasion, but it will eventually stay in that slot.
One of the PolyDryer modifications (which I can no longer find) suggested improving the vent openings, because the default slats block more than half of the surface area:
PolyDryer – molded vent slats
I chopped out all but three of the slats and stuffed an arch of aluminum window screen into each recess:
PolyDryer – vent screens installed
Admittedly, it looks a bit raggedy:
PolyDryer – vent screen – detail
As far as I can tell without actually measuring anything, the air flow has increased.
Now, to see how whether all that makes any difference.
Mary found the wrench I made five years ago in the bottom of her tool bucket:
Hose Valve Knob – five years later
Having moved away from the garden with all the valves that wrench turned, it can now go into the 3D Printed Sample Box for use in the unlikely event I ever give another talk on the subject.
I’d design it differently these days, what with BOSL2 in my sails, but it got the job done.
The Smell of Molten Projects in the Morning 