The Smell of Molten Projects in the Morning

Ed Nisley's Blog: Shop notes, electronics, firmware, machinery, 3D printing, laser cuttery, and curiosities. Contents: 100% human thinking, 0% AI slop.

Category: Science

If you measure something often enough, it becomes science

  • Victoreen 710-104 Ionization Chamber: Gamma Rays!

    Given this hairball circuit:

    Current Amp - Dual Darlington - Schematic
    Current Amp – Dual Darlington – Schematic

    Feeding the output voltage into the ‘scope, with AC coupling to strip off the DC bias, produces this:

    Darlington 12k load - multiple
    Darlington 12k load – multiple

    Those cute little spikes seem to be gamma ray ionization events: they are always positive-going, there are no similar negative-going pulses, they occur irregularly at a few per second with occasional clusters, and generally seem about like random radioactive events. The picture shows a particularly busy interval; mostly, nothing happens and the baseline voltage wobbles around in a low frequency rumble.

    For what it’s worth, the shielding around the circuit completely eliminates not only 60 Hz interference, but everything else, too: astonishingly good results from a fairly simple layout.

    Taking a closer look at one pulse:

    Darl 12k - single detail
    Darl 12k – single detail

    (Vigorous handwaving begins)

    The tallest spikes are typically 20 mV above the baseline, corresponding to peak output current of 20 mV / 12 kΩ = 1.5 µA and a chamber current of 1.5 µA / 100×106 = 15 fA.

    They’re generally 5 ms wide, which is orders of magnitude longer than the actual ion generation time, but the area under that spike should be more-or-less proportional to the area under the actual impulse.

    If you grant that and agree those pulses look mostly triangular, their integral is:

    1/2 x 15 fA x 5 ms = 40 fA·ms = 40 aC

    That’s “a” for “atto” =10-18 = a billionth of a billionth = hardly anything at all.

    Indeed, seeing as how one coulomb contains 6.2×1018 electron charges, that pulse represents 250 ion pairs, at least assuming a zero-current baseline.

    Gamma rays arrive with various energies, produce ionization trails of various lengths, and don’t necessarily traverse the entire chamber, so the pulses have various heights & widths; you can see smaller pulses sticking up out of the grass in the first scope shot. Assuming all those average out to five “big” pulses every second, the chamber collector electrode passes 200 aC/s into the transistor base → 200 aA → 0.20 fA. At 1 fA per 100 µR/h, that’s 20 µR/h of gamma background.

    Frankly, I don’t believe any of that to within an order of magnitude, but given that a free-air monitor counting alpha + beta + gamma background in NYC seems to be averaging 10-ish µR/h, it’s not entirely out of line.

    Working from the other end of the scale, a bit of searching shows that 1 R produces 2.08×109 ion pairs in 1 cm3 of dry air at STP. The ionization chamber dimensions give the can’s volume:

    π x 4.52 x 3.5 = 220 cm3

    So assuming a somewhat unreasonably large pure-gamma dose of 10 µR/h in that volume will produce:

    10x10-6 x 2.08x109 x 220 = 4600x103 ion pairs/h = 1300 ion pairs/s

    That’s about five “big pulses” per second, under the stack of assumptions thus far, and seems absurdly close.

    An old NIST report on Calibration of X-Ray and Gamma-Ray Measuring Instruments says that 1 R/s (that’s per second, not per hour) produces a current of 300 pA/cm3 in an “ideal ionization chamber”. Scaling that down to 10 µR/h and up to the chamber volume gives an average current of 180 aA. That’s absurdly close, too.

    Note bene: Because 1 C = 6.241×1018 ion pairs, 2.08×109 ion pairs is 333×10-12 C and, if you do that in one second, you get 333 pA of current from your ideal 1 cm3 ionization chamber. Those two approaches should be equally close.

    (Vigorous handwaving ends)

    Again, I don’t trust any of the values to within an order of magnitude and surely made a major blunder in running some of the numbers, but the results seem encouraging.

    The coaxial cable’s capacitance could explain why the pulses look like triangles: the capacitance integrates a rectangular current pulse into a voltage ramp. The cable measures 200 pF and the scope input adds 13 pF, but let’s call it 200 pF across the 12 kΩ emitter resistor. Raising the voltage across that capacitance by 20 mV in 2 ms requires a current of:

    200x10-12 x (20 mV / 2 ms) = 2 nA

    Dividing that by 100×106 gives a chamber current pulse of 20×10-18 = 20 aA: three orders of magnitude less than the original guesstimate. That suggests the (handwaved) 15 fA chamber current, amplified by the absurd gain of two stacked Darlingtons, easily drives the cable capacitance. Something else causes the ramp.

    The chamber itself has 10 pF capacitance, but it’s not clear to me how (or if) that enters into the proceedings. The entire collection of ions appears in mid-air, as if by magic, whereupon the +24 V chamber bias voltage draws them (well, the positive ones, anyway) to the transistor base without appreciable voltage change.

    Perhaps the triangle represents the actual arrival of the ions: a few at first from the near side of the trail, a big bunch from the main trail, stragglers from the far side, then tapering off back to the baseline.

    That’s definitely more than anyone should infer from a glitch produced by a pair of transistors…

  • These Are Not the Book Drops You Are Looking For

    The Vassar Library could be a model for J.K. Rowling’s work:

    Vassar Library - front
    Vassar Library – front

    A closer look at the jarringly contemporary containers along the mid-left edge of that picture:

    Vassar Library - Trash and recycling containers
    Vassar Library – Trash and recycling containers

    Pop quiz: How many books did they find in the trash before they added the placards?

    Bonus: How much did that reduce the burn rate? It’s surely still nonzero, because nobody reads instructions. Right?

    Double bonus: Does the real book drop sport a “This is NOT a trash can” placard?

  • Bird Encounter

    At this instant, neither of us realized the other was present:

    Starling-0145
    Starling-0145

    Despite what it looks like, the blackbird (maybe a starling) passed just beyond arm’s reach directly ahead of the bike at eye level:

    Starling-0167
    Starling-0167

    And away!

    Starling-0173
    Starling-0173

    At 60 frames per second, that’s 466 ms of elapsed time.

    Stepping through the video, frame by frame, the bird’s wings flap at a consistent three frames per stroke = 50 ms/stroke = 20 stroke/s = 1200 stroke/min. A bit of rummaging produces a study suggesting a starling’s normal rate is 10 stroke/s, so the critter had the throttles firewalled at war emergency power.

    It makes my pedal pushing seem downright inconsequential…

  • Electrometer Amp: Darlington NPN

    I soldered up the simplest possible “electrometer amplifier” at Squidwrench, based on Charles Wenzel’s writeup:

    Electrometer Amp - MPSA14 NPN Darlington
    Electrometer Amp – MPSA14 NPN Darlington

    It’s an MPSA14 NPN Darlington transistor, with the base soldered directly to the Victoreen 710-104 ionization chamber collector pin. The flying leads connect to an ordinary digital voltmeter set to read voltage, rather than current, so that you see the voltage created by the transistor’s collector current through the meter’s input resistance.

    The MPSA14 data sheet specifies DC current gain hFE > 10 k for low collector currents, with a graph suggesting it might be somewhat larger. Alas, all those are for “ordinary” currents, not the countably finite number of electrons coming from an ionization chamber, but let’s assume 10 k is close.

    I used a Radio Shack 22-805 DMM, set to auto-ranging DC volts. The specs say the input “impedance” is 10 MΩ for all voltage ranges, so let’s run with that, too.

    With 24 V (actually 24.6 V) applied to both the chamber (through the red wire) and the DMM (through the yellow wire), it read 250 mV: a mere 25 nA through the 10 MΩ meter resistance.

    Assuming a transistor gain of 10 k, that’s a chamber current of 2.5 pA.

    The ionization chamber specs say it produces 5 pA at 0.5 röentgen/hour → 100 mR/h produces 1 pA.

    No, I do not believe the Squidwrench Operating Table is bathed in gamma radiation at 250 mR/h.

    I should wipe down the transistor to see if that reduces the external leakage, then try a few others, but obviously the signal will remain lost in the noise.

    We replaced the DMM with an oscilloscope and 10 MΩ probe, which conclusively demonstrated that unshielded high-impedance circuits make excellent 60 Hz receivers.

  • Monthly Science: Mystery Chip

    Dragorn of Kismet gave me a handful of identical mystery chips that might date back to the 1980s. They’re surprisingly large and covered with contacts:

    Mystery IC - overview
    Mystery IC – overview

    There are no logos or identification anywhere on the chip. The back side is blank silicon.

    The visible patterns don’t suggest anything obvious:

    Mystery IC - detail 1
    Mystery IC – detail 1

    The metallization layers aren’t particularly intricate:

    Mystery IC - detail 2
    Mystery IC – detail 2

    Surely there’s something tucked under the top metallization; I have neither the materials nor inclination to dissolve the thing one layer at a time.

    I gave a sampling to our Larval Engineer, who says she may turn them into fancy jewelry. I’m sure the solder bumps contain lead, but …

  • Victoreen 710-104 Ionization Chamber

    Using radiation to generate random numbers reminded me of some Victoreen 710-104 ionization chambers that have been in the pile basically forever:

    Victoreen 710-104 Ionization Chamber
    Victoreen 710-104 Ionization Chamber

    The central contact seems to be double-insulated from the chamber with glass (?) seals in a soldered-in-place assembly:

    Victoreen 710-104 Ionization Chamber - terminal detail
    Victoreen 710-104 Ionization Chamber – terminal detail

    That might be rosin left over from soldering, but you’d think they would have rinsed it off to reduce the leakage. Some cleaning will be in order.

    A picture in The Fine Manual for the CD-V-710 Model 5 Radiation Survey Meter showed that the circuit board used point-to-point wiring, with the range switch soldered directly to that bent metal contact:

    Victoreen CD-V-710 Model 5 Manual - Page 10 - circuit layout
    Victoreen CD-V-710 Model 5 Manual – Page 10 – circuit layout

    Another page gave some useful values and a simplified schematic:

    Victoreen CD-V-710 Model 5 Manual - Page 5
    Victoreen CD-V-710 Model 5 Manual – Page 5

    Never fear, the manual also has the full schematic; they don’t write manuals like that any more.

    The chamber bias voltage was +22.5, from one carbon-zinc battery available back in the 1950s. You can still get 22.5 V batteries at about ten bucks a pop, but 24 V from a pair of cheap & readily available 12 V A23 alkaline batteries should be close enough. There’s no current drain, so the batteries should last their entire shelf life.

    The “HI-MEG” resistor represents a trio of glass-body resistors selected by the range switch:

    • R5 = 100 GΩ → 0.5 R/h
    • R6 = 10 GΩ→ 5 R/h
    • R7 = 1 GΩ→ 50 R/h

    As the saying goes, if you must select R7 in an actual emergency, you should sit down, put your head between your legs, and kiss your ass goodbye.

    The steel-wall chamber responds only to gamma radiation, with a nominal current of 5 pA at 0.5 R/h. However, given an op amp like the LMC6081 with 10 fA bias current, maybe building an electrometer-style amplifier that can respond to background gamma radiation or maybe secondary gamma rays from cosmic ray air showers would be feasible; I haven’t done anything like that in a while and even a faceplant would be interesting.

    Alas, radium-226 and its progeny, including radon-222 decay through alpha and beta emission that’s specifically excluded by the can.

    This is not a new idea, by any means, as shown by some extensive discussion and well-done circuitry. Any amplifier that works with the Victoreen can will certainly work with a homebrew ionization chamber.

  • Fly6 Video Compression: Blur to Sharpen?

    So I stuck a snippet of ordinary “transparent” (it’s actually translucent) adhesive tape across the top of the Cycliq Fly6 camera lens:

    Cycliq Fly6 Camera - blur tape
    Cycliq Fly6 Camera – blur tape

    That smoothly blurs the top third of the frame:

    Fly6 - Tape-blurred frame
    Fly6 – Tape-blurred frame

    The motivation for using translucent tape: it should maintain roughly the same brightness and color balance across the whole image. Opaque tape would burn out the remaining image as the camera desperately tries to maintain an average gray level.

    Fast-forwarding VLC with the video stopped forces it to display the inter-frame compression blocks spanning several seconds of video:

    Fly6 - Forced compression artifacts
    Fly6 – Forced compression artifacts

    The upper third of the frame has big, simple blocks that pegged the files at a uniform 475 MB per ten minute file, somewhat lower than the un-blurred 500 to 700 MB. So the compression definitely isn’t working nearly as hard.

    I hoped that simplifying the uninteresting part of the image would leave more bits for license plates and other interesting details, which might be the case. New York has two main licence plate color schemes (the obsolete high-contrast blue-on-white and the current low-contrast blue-on-orange “Empire Gold”) and both the Fly6 and the Sony AS30V cameras do much better with white plates in full sun.

    Some samples at full size:

    Fly6 - License Plates
    Fly6 – License Plates

    Those were chosen based on:

    • Similar range / angle: just over the center line
    • Same-size crop box: 350 x 197
    • Sun vs. shade

    I think those are somewhat sharper than the plates from un-blurred frames, but it’s not like the camera suddenly woke up smarter and started paying attention to the important stuff.

    Time for more riding, minus the tape…